Pacific Nanotechnology Inc.

Nano-IM™ 6x6 AFM

 

Introduction

The Nano-IMT 6x6 is a complete high performance Atomic Force Microscope system that is optimized for imaging wafers and disks. Applications for the Nano-IMT 6x6 include research, development, process development and process control.
Nano-IM™ 6x6 Stage - Standard 6x6 inch configuration


Included with the system is a master computer, software, an electronic controller, and an AFM stage. The automated X-Y stage accepts wafers up to 6” (150 mm) in diameter and 0.33” (8.5 mm) thick. With this unique stage it is possible to adjust the angle of the probe sample under computer control. Nano-IM™ 6x6 software runs on the Windows XP™ operating system.

The Nano-IM™ 6x6 stage easily fits on a table top and can be operated with high resolution results in a normal laboratory environment.

The stage is designed to maximize flexibility in the types of samples that are accommodated as well as make the setup and alignment of the AFM head as easy as possible.


The stage includes:
• AFM Head
• X-Y Sample Stage Translator
• Sample Stage
• Z Motion Control

All power for the stage is received from the electronic controller via a series of 8’ (2.5 m) long cables. Operation of the stage requires an air pressure line and a vacuum source.

AFM Scanner

The Nano-IM™ 6x6 AFM scanner uses the standard light lever method for monitoring the motion of a cantilever as it is raster scanned across a surface. The scanner is a patented, compact design that offers a direct internal scanner calibration. A hollow pivot scanner facilitates a direct view with a video optical microscope.

Alignment of the AFM sensor is achieved with four adjustment screws that are easily accessed at the front of the AFM head. Two of the adjustments move the laser into position on the cantilever. Two other adjustments move the photo-detector into the path of the reflected laser beam.


Nano-IM™ 6x6 AFM Scanner

Motorized Z Approach

The Nano-IM™ 6x6 includes a unique three motor approach system that is used for moving the AFM probe to the sample for scanning. Each motor has .33” (8.5 mm) of motion, is independently controlled and includes position sensors. The software for activating the Z approach motors is included with the SPMCockpit™ software.


Sample Stage

All types of wafers and disks are accommodated on the Nano-IM™ 6x6 sample stage. After a wafer is placed on the stage, a vacuum is employed to hold the wafer rigidly to the stage. At the surface of the stage are vacuum rings for 2” (50 mm), 4” (101 mm), and 6” (152 mm) diameter wafers. Each of the vacuum rings may be independently activated. Samples having a thickness of up to 0.33” (8.5 mm) may be placed on the sample stage for AFM imaging. The sample stage may be rotated by 360° to image an entire wafer with the AFM without removing the wafer from the stage.

X-Y-Z Sample Stage Translation


The Nano-IM™ 6x6 has a unique design for the X-Y stage translation mechanism. The X-Y motion is generated by stepper motors at the back of the granite support in a position that is not visible, is easily kept clean, and is safe.

The stage has a 6” (150 mm) motion in one direction and a 7” (178 mm) motion in the other. Wafers are easily loaded on the sample stage with software control. Motion of the sample in the Z direction is generated by three motors located inside the gantry. These three motors are useful not only for probe approach, but also for leveling the stage and for precise control of the sample/probe angle.

Software is used for energizing the X-Y sample stage. The window for controlling the stage is illustrated here. The position and rate of travel are software controlled.


Video Optical Microscope


A color video microscope is essential for locating features on a surface for scanning in an AFM. The Nano-IM™ 6x6 AFM has a motorized zoom and focus video microscope controlled by either Nano-IM™ 6x6 AFM software or the system’s trackball. There is a manual control of the X-Y position of the microscope objective for centering the image of the cantilever in the video microscope image.



Optical microscope image of an AFM cantilever in the Nano-I™

Special Nano-IM™ Configurations

The Nano-IM™ AFM is offered to accomodate scanning of non-standard sample shapes and sizes. The AFM scanner is incorporated into a support structure, or gantry, that may be mounted on a customized stage so that almost any size and shape of sample may be scanned successfully.


As an example, Figure 6 illustrates a Nano-IM™ configured for a 12 inch wafer. This stage can also accomodate samples up to 18 inches in diameter.

Nano-IM™ 6x6 Modes

The Nano-IM™ 6x6 system comes with most standard AFM scanning modes. All are controlled by software and work on the provided head. The included modes are:

DC Modes
  Contact Mode Used for basic imaging of a surface
  Lateral Force Mode Image contrast based on surface friction
Vibrating
  Close-Contact Mode Vibrating cantilever with large amplitude
  Non-Contact Mode Vibrating cantilever with small amplitude
  Material Sensing Mode Vibrating cantilever for material contrast
Other
  Force / Distance Mode Force / Distance curves
  Pulsed Force Mode Measures hardness of surface

Controller and Master Computer

The master computer, required for acquiring and analyzing images, is a standard PC type computer. Connection of the computer to the control unit is with a standard Ethernet connecter. Specifications for the computer system are improved on a routine basis when improved computer systems are made available.

AFM Controller


The control unit of the Nano-IM™ 6x6 AFM is based on a PC microcontroller architecture and is connected to the master computer though a standard Ethernet port. Included with the Nano-IM™ 6x6 is a peripheral control cabinet that contains the stage control electronics, a vacuum control system, and a pressure control system. All of the vacuum and pressure hoses required for the vacuum chuck are also included with the Nano-IM™ 6x6 AFM.

For a detailed description of the Nano-IM™ 6x6 controller, request data sheet #P-010-0000-1.



Nano-IM™ Software

There are two software modules for acquiring and analyzing AFM images included with the Nano-IM™ 6x6system. Also available as an option is the Nano-Rule+™ analysis software module. All are described below:

EZMode™ Software: For new users or users that want to use the Nano-IM™ 6x6 on an infrequent basis, EZMode™ software is ideal. EZMode™ software guides an operator through the essential steps for acquiring AFM images.

X’pert™ Mode Software: This acquisition software is designed for advanced users that want the flexibility to control all of the parameters in the Nano-IM™ 6x6 stage. Control of each parameter in the stage is available through a series of windows.

Image Analysis: All of the important features required for rapidly visualizing and analyzing AFM images are included with the Nano-Rule+™ software. Additionally, because Nano-Rule+™ software was written for Windows, it takes advantage of all the state of the art browsing and report generation features available in the Windows environment.


Image Acquisition Software

The Nano-IM™ 6x6 has two types of image capture software; one is for casual or novice users and the other is for advanced users. EZMode™ software is ideal for new Nano-IM™ 6x6 operators or operators that want to use the instrument on an occasional basis. The X’pert™ software gives powerful control over the Nano-IM™ 6x6 and is designed for advanced AFM users.



EZModeTM Software

EZMode™ software is a sequential software package that guides you through the process of acquiring an AFM image. The process oriented software gives a step-by-step procedure for getting an AFM image. At the top of the EZMode™ screen is a sequence of the steps that must be followed.


  • Start: Assure that a cantilever is in the view of the microscope. Place sample in the microscope. Calibrate scanner.
  • Select Mode: Choose contact mode, vibrating mode, or crystal force mode.
  • Align Laser: Align the laser on the cantilever.
  • Frequency Sweep: Perform automatic peak detection for vibrating mode imaging.
  • Stage: Center tip over the area to be scanned.
  • Tip Approach: Activate the motors for approaching the sample with the probe.
  • Scan Sample: Set the scan size and scan parameters.
  • Image Processing: Visualize and analyze images.
  • Tip Retract: Move the tip away from the sample surface.

X’pert™ Mode Software

Direct control of the available features in “interactive” mode is possible with the X’pert™ software. Below is a view of the screen for X’pert™ software . The menu items that are available in the X’pert™ software are:



Oscilloscope Windows

There are five oscilloscope windows for displaying the time variation of a signal, a line, a frequency spectrum, a dual trace scope, and a line scan.

Scanner Control Window
Scanner Control Button: This window is used while scanning a sample. The window shows between 1 and 4 images and has the scan size, speed, PIDsetting, and other scan parameters.
Screen Shot of the Force/Distance Curve Window
Force/Distance Curve Window: Complete control of force/distance curves is possible with the force distance curve window.

Image Analysis

All of the commonly available image analysis techniques come as standard features with the Nano-R™ AFM system. Functions that are available are:

• Histogram Analysis
• Plane Correction
• Image Leveling
• Filter
• 3-D Imaging
• Fast Fourier Transform
• Line Profile


Each of the AFM image analysis software features is activated with an icon at the top of the analysis window.



Software Options

In addition to the software modules provided with the Nano-IMTM system, there are several optional software modules including:

• NanoRule+™
• Grain Analysis
• Particle Analysis
• LPM Software
• DVD

Specifications

Light Lever AFM / Scanner
Force Sensor Light Lever
Detector 4 Quadrant Photo-detector
Laser 650 nm diode – 25 micron spot size
Laser Adjustment 80 TPI
Probe Holder Universal Adapter
Probe Types Pre-mounted - Magnetic
XYZ Calibration Sensors Inductive – 1 nm resolution
Z Scanner Type Piezoelectric Ceramic – Direct
Z Range 8 Microns
Z Noise <0.06 nm*
Z Linearity < 1 %
Z out of plane motion < +/- 30 nm
XY Scanner Type Flexure
XY Range 90 Microns(180 or 360 microns optional)
XY Linearity < 1 %
XY Noise < 0.01 nm (open loop)
XY, XZ, YZ Crosstalk < 1 %
Probe Electrical Connector Isolated 5 Connector

1624 Electronic Control
Scan DAC 16 Bits
XYZ board – Primary and Secondary
• Digital Zoom/Offset
• Analog Zoom
• Z High Voltage
• Z Sample/Hold
• PID Control
• Phase/Amplitude
• XY High Voltage
• XY Sensor Feedback
16 Bits
4 bits on High Voltage
-20 to 140 Volts
20 Bits
Analog
400 Mhz Clock/32 Bit Frequency Control
+X,-X +Y,-Y (-20 to 140 Volts)
Analog PID Control
User Access Connector for Signal Access Console
Internal Digital Control
• CPU
• Operating System
• Communications Protocol
• Memory
Pentium
Linux
TCP/IP
RAM/Disk Drive
Motor Driver Board
• Number of Motor Drivers
• Motor Type
• Control
• Additional Function
7
Stepper
Microprocessor
Light Intensity Control

Stage
XY Stage Range
• X
• Y
150 mm
150 mm
XY Stage Step Size 4 um
XY Stage Accuracy < 10 um
Z Motor Range 8 mm
Z Motor Step Size 162 nm
Sample Puck
• Hold Down
• Height
• Maximum Sample Diameter
Magnetic
30 mm
100 mm
Optical Microscope
• Resolution
• Zoom Ratio
• Field of View
1.5 u
4:1
140 x 190 u at Maximum Zoom
Probe Exchange Flip Up

Physical Specifications
Width Depth Height Weight (kg)
• Stage
• Vibration Enclosure
• Electronic Controller
• Work Station
14 19 16 50
31 33 56 275
12 18 22 22
7 16 16 14

Control Station
Computer Monitor 19” LCD
Video Monitor 19” LCD
Accessories Mouse, Keyboard, Trackball
Computer:
• Type
• Operating System
• Memory
• Disk Drive
AFM Software:
• Acquisition
• Display
Video Converter

IBM PC
Microsoft Vista
> 1 Gigabyte
> 200 G Bytes

EZ Mode™, X’ert™ Mode
AFM Analysis, and NanoRule+™
NTSC – SVGA

Sample Stage
Vacuum Rings 2” (50.8 mm), 4” (101.59 mm),
6” (152.39 mm)
Sample Thickness < 0.3” (8 mm)
Sample Diameter 6” (150 mm) full, < 12” (304.8 mm) partial
Attachment Vacuum

* Vibration environment can lower noise preformance.